The crystal structure of the trans-dimer of 2-methyl-2-nitrosopropane has been established by X-ray diffraction studies. The crystals are monoclinic, space group P21/n, with Z= 2 and unit-cell constants a= 5.929 0(18), b= 10.112(3), c= 8.751(4)Å, and β= 90.80(3)°. Although the NN- and ON-bond distances are normal for nitroso compounds, the CN-distance was significantly longer than expected.
B. G. Gowenlock, K. J. McCullough and R. B. Manson, J. Chem. Soc., Perkin Trans. 2, 1988, 701 DOI: 10.1039/P29880000701
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