The new complex K4[MoH(CN)7]·2H2O and its characterisation by 1H, 13C n.m.r. and vibrational spectra are reported. Vibrational and n.m.r. data are also presented for [MH(CN)5]3–(M = Rh or Ir). Attempts to prepare other cyanide hydride species are discussed. Reactions of the above species with small molecules and unsaturated hydrocarbons are reported.
M. J. Mockford and W. P. Griffith, J. Chem. Soc., Dalton Trans., 1985, 717 DOI: 10.1039/DT9850000717
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