Reaction of a di-copper(II) complex of a macrocyclic ligand with acetonitrile in the presence of O2 and H2O affords a pentanuclear complex containing two-co-ordinate and three-co-ordinate copper(I) atoms linked via triply bridging 3,5-dimethyl-1,2,4-triazolate groups.
M. G. B. Drew, P. C. Yates, J. Trocha-Grimshaw, K. P. McKillop and S. M. Nelson, J. Chem. Soc., Chem. Commun., 1985, 262 DOI: 10.1039/C39850000262
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