Reduction of optically pure acyl-lactones (2) by L-Selectride affords monoprotected syn diols with high diastereoselectivity; the reaction was applied to the stereo- and enantio-specific synthesis of (+)-exobrevicomin.
M. Larchevêque and J. Lalande, J. Chem. Soc., Chem. Commun., 1985, 83 DOI: 10.1039/C39850000083
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