Two-step hydrolithiation of 3,4,6-tri-O-benzyl-D-glucal (hydrochlorination and lithium naphthalenide reductive lithiation) gives a reactive glycosyl-lithium derivative which is shown to be a precursor of C-glycosides.
J. Lancelin, L. Morin-Allory and P. Sinaÿ, J. Chem. Soc., Chem. Commun., 1984, 355 DOI: 10.1039/C39840000355
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