3-Lithio-1-methoxybutane is tetrameric in benzene and crystallizes as the chelated meso-tetramer whose increased C–Li and decreased Li–Li distances reflect the size of the organic group.
G. W. Klumpp, P. J. A. Geurink, A. L. Spek and A. J. M. Duisenberg, J. Chem. Soc., Chem. Commun., 1983, 814 DOI: 10.1039/C39830000814
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