The rhodium dimer, (CO)2(PPh3)Rh(µ-CO)2Rh(PPh3)2(CO) has been synthesized by treating anionic rhodium carbonyl complexes containing triphenylphosphine ligands with methanol; the molecular structure of this complex has been determined by single crystal X-ray diffraction.
A. S. C. Chan, H. Shieh and J. R. Hill, J. Chem. Soc., Chem. Commun., 1983, 688 DOI: 10.1039/C39830000688
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