The first total synthesis of the polyoxygenated diterpene insect antifeedant ajugarin I (1) has been achieved by a route which involves a new method for the construction of 3-substituted-Δ2-butenolides.
S. V. Ley, N. S. Simpkins and A. J. Whittle, J. Chem. Soc., Chem. Commun., 1983, 503 DOI: 10.1039/C39830000503
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