[2,8-2H2]Oct-1-ene, with 98% and 93% deuterium incorporation at C-2 and C-8, respectively, is prepared from 6-bromohexan-1-ol in a six-step synthesis which offers access to a wide range of ω-labelled acyclic aliphatic compounds.
G. Read and I. Townsend, J. Chem. Soc., Perkin Trans. 1, 1982, 2901 DOI: 10.1039/P19820002901
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