Polydiacetylene films and powders have been prepared from the AsF5-induced polymerization of butadiyne in both the solid and gas phases at low temperatures; the charge transfer interaction can be explosive if large quantities of the reactants are mixed.
P. J. Russo and M. M. Labes, J. Chem. Soc., Chem. Commun., 1982, 53 DOI: 10.1039/C39820000053
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