Electrogeneration of manganese(II) at platinum, gold and glassy carbon was investigated by rotating disc electrode voltammetry. Anodic charge-transfer kinetic parameters were determined and used to compute generation current efficiencies. The maximum value obtained was 99.91% at a generating current density of 8.95 mA cm–2, in sulphuric acid. The most appropriate electrode material is gold.
E. Bishop and P. Cofré, Analyst, 1981, 106, 429 DOI: 10.1039/AN9810600429
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