The ketols (1a)–(3a), have been prepared and barriers for degenerate rearrangement, by intramolecular hydride transfer, in the derived sodium alkoxides, (1b)–(3b) have been determined from their temperature dependent 13C n.m.r. spectra.
G. Craze and I. Watt, J. Chem. Soc., Chem. Commun., 1980, 147 DOI: 10.1039/C39800000147
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