Phosphonic acid dialkyl esters are transformed in high yield into the corresponding bistrimethylsilyl esters on treatment with iodotrimethylsilane; subsequent hydrolysis of these products affords the parent phosphonic acids under mild conditions without influence on a variety of other functional groups.
G. M. Blackburn and D. Ingleson, J. Chem. Soc., Chem. Commun., 1978, 870 DOI: 10.1039/C39780000870
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