The first synthesis of an unsymmetrical tetrathiafulvalene derivative by a mixed coupling reaction has been achieved; the resulting diester (7) has been demethoxycarbonylated to the highly unsymmetrical benzotetrathiafulvalene (8).
H. K. Spencer, M. P. Cava and A. F. Garito, J. Chem. Soc., Chem. Commun., 1976, 966 DOI: 10.1039/C39760000966
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