The [Rh13(CO)24H5–n]n–(n= 2 or 3) anions have been isolated from the reaction of the [Rh12(CO)30]2– dianion with hydrogen; they are structurally related to a close hexagonal packing of rhodium atoms having mean distances of 2.81 Å.
V. G. Albano, A. Ceriotti, P. Chini, G. Ciani, S. Martinengo and W. M. Anker, J. Chem. Soc., Chem. Commun., 1975, 859 DOI: 10.1039/C39750000859
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