Reaction of Re(CO)5NO3 with Ph4As+NO3– yields the compound Ph4As+[Re(CO)4(NO3)2]– incorporating the first reported example of a mononuclear dinitratocarbonylmetallate. I.r. spectroscopy indicates unidentate nitrate ligands in cis-configuration.
C. C. Addison, R. Davis and N. Logan, J. Chem. Soc., Dalton Trans., 1974, 1073 DOI: 10.1039/DT9740001073
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