Sterically hindered alcohols e.g.(I; R = H) were acylated with O-4-methylphenyl chlorothioformate in high yield and the resulting thiocarbonates were converted into olefins by pyrolysis.
H. Gerlach, T. T. Houng and W. Müller, J. Chem. Soc., Chem. Commun., 1972, 1215 DOI: 10.1039/C39720001215
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