A single-crystal X-ray study has shown the NiII complex of cis,cis-1,3,5-tris(pyridine-2-aldimino)-cyclohexane to have a geometry intermediate between trigonal prismatic and octahedral, with an average angle of twist from trigonal prismatic of approximately 32°.
E. B. Fleischer, A. E. Gebala and D. R. Swift, J. Chem. Soc. D, 1971, 1280 DOI: 10.1039/C29710001280
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