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A novel cobalt(0) alkyne complex assisted “capture and release” strategy for oligosaccharide rapid assembly

Abstract

A chromatographic-purification free rapid oligosaccharide synthetic strategy was developed. The intermediates were conveniently purified by a new process based on “capture-release” strategy on resin that involved the Co2(CO)6-PPh2/alkyne complex and oxidated de-complex reaction. This method eased the redundant muti-steps classical chromatographic purification protocol and has been proved to be efficient by the synthesis of linear and branched penta-mannosides.

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Publication details

The article was received on 28 Mar 2018, accepted on 16 May 2018 and first published on 17 May 2018


Article type: Research Article
DOI: 10.1039/C8QO00324F
Citation: Org. Chem. Front., 2018, Accepted Manuscript
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    A novel cobalt(0) alkyne complex assisted “capture and release” strategy for oligosaccharide rapid assembly

    Y. Liu, Y. Wang, S. Meng, X. Meng, Z. Li and Q. Lou, Org. Chem. Front., 2018, Accepted Manuscript , DOI: 10.1039/C8QO00324F

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