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Issue 7, 2018
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Synthesis of fullerotetrahydropyridazines via the copper-catalyzed heteroannulation of [60]fullerene with hydrazides

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Abstract

A series of novel fullerotetrahydropyridazines have been prepared via the reaction of [60]fullerene with hydrazides catalyzed by cheap and readily available Cu(OAc)2·H2O. This protocol features a broad substrate scope and good functional group tolerance. A possible reaction mechanism for the formation of fullerotetrahydropyridazines is proposed on the basis of the experimental results. The electrochemistry of the obtained products has also been investigated.

Graphical abstract: Synthesis of fullerotetrahydropyridazines via the copper-catalyzed heteroannulation of [60]fullerene with hydrazides

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Publication details

The article was received on 17 Nov 2017, accepted on 26 Jan 2018 and first published on 29 Jan 2018


Article type: Research Article
DOI: 10.1039/C7QO01032J
Citation: Org. Chem. Front., 2018,5, 1188-1193
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    Synthesis of fullerotetrahydropyridazines via the copper-catalyzed heteroannulation of [60]fullerene with hydrazides

    S. Jiang, Z. Liu, W. Lu and G. Wang, Org. Chem. Front., 2018, 5, 1188
    DOI: 10.1039/C7QO01032J

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