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Issue 5, 2018
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A more sustainable and efficient access to IMes·HCl and IPr·HCl by ball-milling

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Abstract

Herein is described a mechanochemical one-pot two-step procedure giving access to various NHC (N-heterocyclic carbene) precursors. This original approach enabled the production of the widely used IPr·HCl, IMes·HCl, Io-Tol·HCl and ICy·HCl in much better yields than conventional solvent-based procedures, while the environmental impact was drastically reduced.

Graphical abstract: A more sustainable and efficient access to IMes·HCl and IPr·HCl by ball-milling

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Publication details

The article was received on 23 Nov 2017, accepted on 27 Dec 2017 and first published on 02 Jan 2018


Article type: Communication
DOI: 10.1039/C7GC03539J
Citation: Green Chem., 2018,20, 964-968
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    A more sustainable and efficient access to IMes·HCl and IPr·HCl by ball-milling

    A. Beillard, X. Bantreil, T. Métro, J. Martinez and F. Lamaty, Green Chem., 2018, 20, 964
    DOI: 10.1039/C7GC03539J

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