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Multinuclear solid-state NMR study: a powerful tool for understanding the structure of ZnO hybrid nanoparticles

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Abstract

Characterization of hybrid materials is crucial for gaining an in-depth understanding of nano-objects. Here, it is evidenced that the use of multinuclear 1H, 2H, 13C, 15N, 67Zn and 17O MAS NMR spectroscopy is a very powerful approach to acquire both structural and dynamic information on hybrid ZnO nanomaterials prepared from an organometallic approach. Not only is the coordination mode of the organic part onto the inorganic surface evidenced but also important information about the dynamics of the organic capping molecules and some particularities of the nanocrystal structure itself are obtained.

Graphical abstract: Multinuclear solid-state NMR study: a powerful tool for understanding the structure of ZnO hybrid nanoparticles

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Publication details

The article was received on 16 Feb 2018, accepted on 05 Apr 2018 and first published on 05 Apr 2018


Article type: Paper
DOI: 10.1039/C8CP01096J
Citation: Phys. Chem. Chem. Phys., 2018, Advance Article
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    Multinuclear solid-state NMR study: a powerful tool for understanding the structure of ZnO hybrid nanoparticles

    G. Spataro, Y. Champouret, P. Florian, Y. Coppel and M. L. Kahn, Phys. Chem. Chem. Phys., 2018, Advance Article , DOI: 10.1039/C8CP01096J

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