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Issue 34, 2018
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Enhanced measurement of residual chemical shift anisotropy for small molecule structure elucidation

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Abstract

A method is introduced to measure residual chemical shift anisotropies conveniently and accurately in the mesophase of poly-γ-(benzyl-L-glutamate). The alignment amplitude is substantially enhanced over common methods which greatly benefits measurements particularly on sp3 carbons. The approach offers significant improvements in data accuracy and utility for small molecule structure determination.

Graphical abstract: Enhanced measurement of residual chemical shift anisotropy for small molecule structure elucidation

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Publication details

The article was received on 22 Jan 2018, accepted on 31 Jan 2018 and first published on 05 Mar 2018


Article type: Communication
DOI: 10.1039/C8CC00552D
Citation: Chem. Commun., 2018,54, 4254-4257
  • Open access: Creative Commons BY-NC license
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    Enhanced measurement of residual chemical shift anisotropy for small molecule structure elucidation

    Y. Liu, R. D. Cohen, K. R. Gustafson, G. E. Martin and R. T. Williamson, Chem. Commun., 2018, 54, 4254
    DOI: 10.1039/C8CC00552D

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