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Issue 5, 2018
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High throughput mechanochemistry: application to parallel synthesis of benzoxazines

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Abstract

We describe herein an unprecedented mechanochemical “parallel synthesis” of 3,4-dihydro-2H-benzo[e][1,3]oxazine derivatives via a one pot three component reaction. The new milling system uses a multiposition jar (variable sizes are possible), allowing for the processing of up to 12 samples simultaneously, leading to the formation of a fungicide and a building block for polymer preparation with higher throughput compared to standard milling devices.

Graphical abstract: High throughput mechanochemistry: application to parallel synthesis of benzoxazines

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Publication details

The article was received on 09 Oct 2017, accepted on 12 Dec 2017 and first published on 12 Dec 2017


Article type: Communication
DOI: 10.1039/C7CC07758K
Citation: Chem. Commun., 2018,54, 551-554
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    High throughput mechanochemistry: application to parallel synthesis of benzoxazines

    K. Martina, L. Rotolo, A. Porcheddu, F. Delogu, S. R. Bysouth, G. Cravotto and E. Colacino, Chem. Commun., 2018, 54, 551
    DOI: 10.1039/C7CC07758K

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