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Issue 12, 2017
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One-step solid state reaction for the synthesis of ternary nitrides Co3Mo3N and Fe3Mo3N

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Abstract

Intermetallic ternary Mo-nitrides are important functional materials due to their unique physical and chemical properties. However, the preparation of this class of materials is usually divided into two steps: the first step is the preparation of the ternary oxides, the second step is the nitridation of the ternary oxides. In this study, a facile procedure for synthesizing ternary Mo-nitrides has been reported. Co3Mo3N and Fe3Mo3N nanoparticles have been synthesized by a one step solid state reaction in a sealed autoclave at 750 °C. The structures and morphologies of the obtained products are derived from X-ray diffraction and electron microscopy. Furthermore, the oxidation resistances and magnetic properties of the obtained products have been investigated.

Graphical abstract: One-step solid state reaction for the synthesis of ternary nitrides Co3Mo3N and Fe3Mo3N

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Publication details

The article was received on 30 Jul 2017, accepted on 01 Oct 2017 and first published on 12 Oct 2017


Article type: Research Article
DOI: 10.1039/C7QI00447H
Citation: Inorg. Chem. Front., 2017,4, 2055-2058
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    One-step solid state reaction for the synthesis of ternary nitrides Co3Mo3N and Fe3Mo3N

    L. Wang, W. Xian, K. Zhang, W. Liu, H. Qin, Q. Zhou and Y. Qian, Inorg. Chem. Front., 2017, 4, 2055
    DOI: 10.1039/C7QI00447H

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