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One-step solid state reaction for the synthesis of ternary nitrides Co3Mo3N and Fe3Mo3N

Abstract

Intermetallic ternary Mo-nitrides are important functional materials for their unique physical and chemical properties. However, the preparation of this class materials is usually divided into two steps: the first step is the preparation of the ternary oxides, the second step is nitridation of the ternary oxides. In this study, a facile procedure for synthesizing ternary Mo-nitrides has been reported. Co3Mo3N and Fe3Mo3N nanoparticles have been synthesized by one step solid state reaction in a sealed autoclave at 750 °C. The structures and morphologies of the obtained products are derived from X-ray diffraction and electron microscopy. Furthermore, the oxidation resistances and magnetic properties of the obtained products have been investigated.

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Publication details

The article was received on 30 Jul 2017, accepted on 01 Oct 2017 and first published on 12 Oct 2017


Article type: Research Article
DOI: 10.1039/C7QI00447H
Citation: Inorg. Chem. Front., 2017, Accepted Manuscript
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    One-step solid state reaction for the synthesis of ternary nitrides Co3Mo3N and Fe3Mo3N

    L. Wang, W. Xian, K. Zhang, H. Qin, W. Liu, Q. Zhou and Y. Qian, Inorg. Chem. Front., 2017, Accepted Manuscript , DOI: 10.1039/C7QI00447H

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