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Issue 37, 2017
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Microwave-assisted synthesis of novel hetero[5]helicene-like molecules and coumarin derivatives

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Abstract

A concise and efficient approach to design and synthesize hetero[5]helicene-like molecules and coumarin derivatives is reported. Intriguingly, using the same catalyst (silica sulfuric acid), and a different solvent and reaction temperature, the reaction selectively afforded hetero[5]helicene-like molecules 3 or coumarin derivatives 4. Product 4 has a highly planar geometry, and product 3 can be regarded as hetero[5]helicene-like because of its helical conformation.

Graphical abstract: Microwave-assisted synthesis of novel hetero[5]helicene-like molecules and coumarin derivatives

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Publication details

The article was received on 15 Jul 2017, accepted on 30 Aug 2017 and first published on 30 Aug 2017


Article type: Paper
DOI: 10.1039/C7OB01742A
Citation: Org. Biomol. Chem., 2017,15, 7909-7916
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    Microwave-assisted synthesis of novel hetero[5]helicene-like molecules and coumarin derivatives

    W. Lin, X. Hu, S. Song, Q. Cai, Y. Wang and D. Shi, Org. Biomol. Chem., 2017, 15, 7909
    DOI: 10.1039/C7OB01742A

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