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Photochemical Studies on Bis-Sulfide and -Sulfone Tethered Polyenic Derivatives

Abstract

This study focusses on the [2+2]-photocycloaddition of symmetric polyenic system tethered by an aryl bis-sulfide or sulfone platform. Using direct irradiation or photosensibilization, no expected ladderane product was isolated. In most cases, only tricyclic products including a single cyclobutane moeity were formed. Irradiation of bis-acrylic precursors in water with encapsulation by a host (cyclodextrin or cucurbituril) provided a stereoselective access to valuable cyclobutyl adducts.

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Publication details

The article was received on 03 Mar 2017, accepted on 05 Apr 2017 and first published on 05 Apr 2017


Article type: Paper
DOI: 10.1039/C7OB00551B
Citation: Org. Biomol. Chem., 2017, Accepted Manuscript
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    Photochemical Studies on Bis-Sulfide and -Sulfone Tethered Polyenic Derivatives

    L. Fensterbank, S. Guelen, M. Blazejak, L. Chamoreau, H. Arnaud, S. Derenne, F. Volatron and V. Mansuy, Org. Biomol. Chem., 2017, Accepted Manuscript , DOI: 10.1039/C7OB00551B

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