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Issue 13, 2017
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Efficient synthesis of aliphatic sulfones by Mg mediated coupling reactions of sulfonyl chlorides and aliphatic halides

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Abstract

Sulfonyl chlorides were reduced to anhydrous sulfinate salts with magnesium under sonication. These sulfinates were alkylated to sulfones with alkyl chlorides in the presence of catalytic sodium iodide under sonication. A variety of aliphatic sulfones was efficiently prepared by this one-pot two-step procedure.

Graphical abstract: Efficient synthesis of aliphatic sulfones by Mg mediated coupling reactions of sulfonyl chlorides and aliphatic halides

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Publication details

The article was received on 01 Feb 2017, accepted on 07 Mar 2017 and first published on 07 Mar 2017


Article type: Paper
DOI: 10.1039/C7OB00251C
Citation: Org. Biomol. Chem., 2017,15, 2841-2845
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    Efficient synthesis of aliphatic sulfones by Mg mediated coupling reactions of sulfonyl chlorides and aliphatic halides

    Y. Fu, Q. Xu, Q. Li, Z. Du, K. Wang, D. Huang and Y. Hu, Org. Biomol. Chem., 2017, 15, 2841
    DOI: 10.1039/C7OB00251C

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