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A facile and green synthesis of MIL-100(Fe) with high-yield and its catalytic performance

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Abstract

MIL-100(Fe) is one of the important metal–organic frameworks due to its fascinating physicochemical properties. Generally, MIL-100(Fe) was synthesized under the conditions of adding HF and solvent. Here, we report that MIL-100(Fe) can be facilely synthesized without the addition of solvent and HF. More importantly, this approach can produce MIL-100(Fe) with a high yield of 93%. Additionally, the obtained MIL-100(Fe) exhibited good catalytic performance in the acetalization of benzaldehyde with methanol. This catalyst can still maintain the initial catalytic activity after five cycles.

Graphical abstract: A facile and green synthesis of MIL-100(Fe) with high-yield and its catalytic performance

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Publication details

The article was received on 11 Aug 2017, accepted on 26 Sep 2017 and first published on 27 Sep 2017


Article type: Paper
DOI: 10.1039/C7NJ02975F
Citation: New J. Chem., 2017, Advance Article
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    A facile and green synthesis of MIL-100(Fe) with high-yield and its catalytic performance

    L. Han, H. Qi, D. Zhang, G. Ye, W. Zhou, C. Hou, W. Xu and Y. Sun, New J. Chem., 2017, Advance Article , DOI: 10.1039/C7NJ02975F

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