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Issue 9, 2017
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An efficient synthesis of nitrile, tetrazole and urea from carbonyl compounds

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Abstract

An efficient conversion of carbonyl compounds (aldehydes and ketones) to nitrile, tetrazole, and urea was developed with the use of a POCl3 and sodium azide mixture using a convergent and microwave method. This is the first report on the direct conversion of ketone to urea. The synthesized compounds were characterized by 1H NMR, 13C NMR, mass and IR spectroscopies and were found to be in agreement with reported compounds.

Graphical abstract: An efficient synthesis of nitrile, tetrazole and urea from carbonyl compounds

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Publication details

The article was received on 09 Dec 2016, accepted on 22 Mar 2017 and first published on 07 Apr 2017


Article type: Paper
DOI: 10.1039/C6NJ03860C
Citation: New J. Chem., 2017,41, 3414-3421
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    An efficient synthesis of nitrile, tetrazole and urea from carbonyl compounds

    R. Sribalan, A. Sangili, G. Banuppriya and V. Padmini, New J. Chem., 2017, 41, 3414
    DOI: 10.1039/C6NJ03860C

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