First synthesis of heterocyclic allenes – benzazecine derivatives

Leonid G. Voskressensky; Alexander A. Titov; Maksad S. Dzhankaziev; Tatiana N. Borisova; Maxim S. Kobzev; Pavel V. Dorovatovskii; Victor N. Khrustalev; Alexander V. Aksenov; Alexey V. Varlamov

doi:10.1039/C6NJ03403A

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First synthesis of heterocyclic allenes – benzazecine derivatives†

Leonid G. Voskressensky,

*^a Alexander A. Titov,^a Maksad S. Dzhankaziev,^a Tatiana N. Borisova,^a Maxim S. Kobzev,^a Pavel V. Dorovatovskii,^b Victor N. Khrustalev,^ac Alexander V. Aksenov

^d and Alexey V. Varlamov^a

Author affiliations

* Corresponding authors

^a Organic Chemistry Department, Peoples' Friendship University of Russia, 6 Miklukho-Maklaya St., Moscow 117198, Russia
E-mail: lvoskressensky@sci.pfu.edu.ru

^b National Research Center “Kurchatov Institute”, 1, Akademika Kurchatova pl., Moscow 123182, Russia

^c Nesmeyanov Institute of Organoelement Compounds of RAS, 28, Vavilova St., GSP-1, Moscow 119991, Russia

^d North-Caucasus Federal University, 1, Pushkin Street, Stavropol 355009, Russia

Abstract

Benzazecines with an allene fragment were prepared for the first time and in high yields via tandem reaction of 1-phenylethynyl-1-methyl(benzyl)-1,2,3,4-tetrahydroisoquinolines with activated alkynes in trifluoroethanol.

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DOI: https://doi.org/10.1039/C6NJ03403A
Article type: Letter
Submitted: 29 Oct 2016
Accepted: 13 Jan 2017
First published: 16 Jan 2017
This article is Open Access

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New J. Chem., 2017,41, 1902-1904

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First synthesis of heterocyclic allenes – benzazecine derivatives

L. G. Voskressensky, A. A. Titov, M. S. Dzhankaziev, T. N. Borisova, M. S. Kobzev, P. V. Dorovatovskii, V. N. Khrustalev, A. V. Aksenov and A. V. Varlamov, New J. Chem., 2017, 41, 1902 DOI: 10.1039/C6NJ03403A

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New Journal of Chemistry

First synthesis of heterocyclic allenes – benzazecine derivatives†

Abstract

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First synthesis of heterocyclic allenes – benzazecine derivatives

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