Issue 20, 2017

A new, low impact and efficient synthesis of ω-nitro esters under solid heterogeneous catalysis

Abstract

Herein, we report a new, efficient and sustainable synthetic protocol for the preparation of ω-nitro esters starting from cyclic 2-nitro ketones. The method involves the use of polymer bound BEMP and provides the target compounds in excellent yields and low process mass intensity and E-factor values.

Graphical abstract: A new, low impact and efficient synthesis of ω-nitro esters under solid heterogeneous catalysis

Supplementary files

Article information

Article type
Paper
Submitted
24 Jul 2017
Accepted
12 Sep 2017
First published
12 Sep 2017

Green Chem., 2017,19, 4956-4960

A new, low impact and efficient synthesis of ω-nitro esters under solid heterogeneous catalysis

E. Chiurchiù, S. Gabrielli, R. Ballini and A. Palmieri, Green Chem., 2017, 19, 4956 DOI: 10.1039/C7GC02241G

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