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Benign-by-design preparation of iron oxides/humins catalytic nanocomposites

Abstract

The current acid-catalyzed conversion of biomass feedstocks yields substantial quantities of undesired by-products called humins, for which applications has yet to be found. This work aims to provide a starting point for humins valorisation via preparation of humin-based iron oxide catalytic nanocomposites from humins and thermally treated humins (foams) via solvent-free methodologies including ball milling and thermal degradation. The prepared materials were found to be active in the microwave-assisted selective oxidation of isoeugenol (conversions ca. 60-90%) to vanillin, proving the feasibility to use humin by-products as template/composite materials.

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Publication details

The article was received on 12 May 2017, accepted on 09 Aug 2017 and first published on 09 Aug 2017


Article type: Paper
DOI: 10.1039/C7GC01405H
Citation: Green Chem., 2017, Accepted Manuscript
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    Benign-by-design preparation of iron oxides/humins catalytic nanocomposites

    L. Filiciotto, A. M. M. Balu, A. A. Romero, E. Rodriguez-Castellón, J. K. van der Waal and R. Luque, Green Chem., 2017, Accepted Manuscript , DOI: 10.1039/C7GC01405H

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