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The Cu(I)-catalysed Huisgen 1,3-dipolar cycloaddition route to (bio-)organic functionalisation of polyoxovanadates

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Abstract

The [V6O13{(OCH2)3CCH2OCH2C[triple bond, length as m-dash]CH}2]2− with two terminal alkyne functionalities exhibits excellent reactivity towards (bio-)organic azides. The designed synthetic protocol for the generation of triazol-modified Lindqvist hexavanadates grants access to bio-“clicked” polyoxometalates with spectroscopically detectable 51V nuclei.

Graphical abstract: The Cu(i)-catalysed Huisgen 1,3-dipolar cycloaddition route to (bio-)organic functionalisation of polyoxovanadates

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Publication details

The article was received on 11 Sep 2017, accepted on 21 Sep 2017 and first published on 22 Sep 2017


Article type: Communication
DOI: 10.1039/C7DT03376A
Citation: Dalton Trans., 2017, Advance Article
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    The Cu(I)-catalysed Huisgen 1,3-dipolar cycloaddition route to (bio-)organic functionalisation of polyoxovanadates

    O. Linnenberg, A. Kondinski, C. Stöcker and K. Yu. Monakhov, Dalton Trans., 2017, Advance Article , DOI: 10.1039/C7DT03376A

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