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Issue 21, 2017
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High-throughput evaluation of in situ-generated cobalt(III) catalysts for acyl fluoride synthesis

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Abstract

Using a high-throughput experimental procedure, a series of cobalt(III) complexes of the general formula CpRCo(I)(X)(L) were prepared and screened for their activity towards the catalytic nucleophilic fluorination of benzoyl chloride. A highly active catalyst was identified, and successfully employed in a mild and effective protocol for the synthesis of a group of acyl fluoride compounds.

Graphical abstract: High-throughput evaluation of in situ-generated cobalt(iii) catalysts for acyl fluoride synthesis

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Publication details

The article was received on 27 Jul 2017, accepted on 04 Oct 2017 and first published on 04 Oct 2017


Article type: Paper
DOI: 10.1039/C7CY01519D
Citation: Catal. Sci. Technol., 2017,7, 4996-5003
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    High-throughput evaluation of in situ-generated cobalt(III) catalysts for acyl fluoride synthesis

    G. M. Lee, R. Clément and R. Tom Baker, Catal. Sci. Technol., 2017, 7, 4996
    DOI: 10.1039/C7CY01519D

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