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Issue 12, 2017
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Room temperature silylation of alcohols catalyzed by metal organic frameworks

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Abstract

The commercial Al(OH)(BDC) (BDC: 1,4-benzenedicarboxylic acid) metal organic framework (Basolite A100) is a suitable heterogeneous catalyst for the silylation of benzylic and aliphatic alcohols by hexamethyldisilazane in toluene at room temperature. Al(OH)(BDC) is stable under the reaction conditions as evidenced by powder XRD and can be reused with minimal activity decrease.

Graphical abstract: Room temperature silylation of alcohols catalyzed by metal organic frameworks

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Publication details

The article was received on 27 Apr 2017, accepted on 23 May 2017 and first published on 24 May 2017


Article type: Communication
DOI: 10.1039/C7CY00834A
Citation: Catal. Sci. Technol., 2017,7, 2445-2449
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    Room temperature silylation of alcohols catalyzed by metal organic frameworks

    A. Dhakshinamoorthy, A. Santiago-Portillo, P. Concepción, J. R. Herance, S. Navalón, M. Alvaro and H. Garcia, Catal. Sci. Technol., 2017, 7, 2445
    DOI: 10.1039/C7CY00834A

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