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Issue 77, 2017
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Harnessing sunlight without a photosensitizer for highly efficient consecutive [3+2]/[4+2] annulation to synthesize fused benzobicyclic skeletons

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Abstract

A photosensitizer-free, highly efficient sunlight-promoted tandem [3+2]/[4+2] annulation of unsaturated α-bromocarbonyls with o-alkynylanilines was developed, and allowed for convenient synthesis of fused benzobicyclic skeletons. The reaction was clean and practical in mild conditions and showed excellent functional group compatibility.

Graphical abstract: Harnessing sunlight without a photosensitizer for highly efficient consecutive [3+2]/[4+2] annulation to synthesize fused benzobicyclic skeletons

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Publication details

The article was received on 20 Aug 2017, accepted on 07 Sep 2017 and first published on 07 Sep 2017


Article type: Communication
DOI: 10.1039/C7CC06548E
Citation: Chem. Commun., 2017,53, 10707-10710
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    Harnessing sunlight without a photosensitizer for highly efficient consecutive [3+2]/[4+2] annulation to synthesize fused benzobicyclic skeletons

    N. Zhou, Y. Cheng, J. Xie and C. Zhu, Chem. Commun., 2017, 53, 10707
    DOI: 10.1039/C7CC06548E

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