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Solvent-free on-surface synthesis of boroxine COF monolayers

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Abstract

A protocol is proposed for the solvent-free on-surface synthesis of covalent organic framework monolayers by condensation of diboronic acids. Monomers are vapor-deposited and water is used for equilibrium regulation. Samples are characterized on progressively smaller length scales by light microscopy, Scanning Electron Microscopy, and Scanning Tunneling Microscopy.

Graphical abstract: Solvent-free on-surface synthesis of boroxine COF monolayers

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Publication details

The article was received on 13 Feb 2017, accepted on 11 Apr 2017 and first published on 12 Apr 2017


Article type: Communication
DOI: 10.1039/C7CC01131H
Citation: Chem. Commun., 2017, Advance Article
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    Solvent-free on-surface synthesis of boroxine COF monolayers

    S. Spitzer, A. Rastgoo-Lahrood, K. Macknapp, V. Ritter, S. Sotier, W. M. Heckl and M. Lackinger, Chem. Commun., 2017, Advance Article , DOI: 10.1039/C7CC01131H

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