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Issue 44, 2016
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Highly regioselective synthesis of 4-tosylthiomorpholine via intramolecular cyclization of N-tethered thioalkenols

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Abstract

A one-pot, metal-free procedure has been developed for the synthesis of 4-tosylthiomorpholine from N-tethered thioalkenols via bromination, cyclization and subsequent elimination reaction in good yields. The reaction is found to be highly regioselective.

Graphical abstract: Highly regioselective synthesis of 4-tosylthiomorpholine via intramolecular cyclization of N-tethered thioalkenols

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Publication details

The article was received on 25 Aug 2016, accepted on 12 Oct 2016 and first published on 13 Oct 2016


Article type: Paper
DOI: 10.1039/C6OB01869F
Citation: Org. Biomol. Chem., 2016,14, 10489-10495
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    Highly regioselective synthesis of 4-tosylthiomorpholine via intramolecular cyclization of N-tethered thioalkenols

    A. K. Saikia, M. J. Deka and U. Borthakur, Org. Biomol. Chem., 2016, 14, 10489
    DOI: 10.1039/C6OB01869F

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