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Issue 22, 2016
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An unprecedentedly simple method of synthesis of aryl azides and 3-hydroxytriazenes

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Abstract

Fischer's approach towards the synthesis of aryl azides and triazinoles from diazonium salts and hydroxylammonium chloride (phenylhydraxylamine) was reinvestigated and optimized. The new methodology enables the preparation of aryl azides and triazinoles in high yields in water at room temperature. The procedure is very simple, robust, easily scalable, reproducible, and “green”.

Graphical abstract: An unprecedentedly simple method of synthesis of aryl azides and 3-hydroxytriazenes

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Publication details

The article was received on 25 Aug 2016, accepted on 30 Sep 2016 and first published on 30 Sep 2016


Article type: Communication
DOI: 10.1039/C6GC02379G
Citation: Green Chem., 2016,18, 5984-5988
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    An unprecedentedly simple method of synthesis of aryl azides and 3-hydroxytriazenes

    P. S. Gribanov, M. A. Topchiy, Y. D. Golenko, Y. I. Lichtenstein, A. V. Eshtukov, V. E. Terekhov, A. F. Asachenko and M. S. Nechaev, Green Chem., 2016, 18, 5984
    DOI: 10.1039/C6GC02379G

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