Guidance from an in situ hot stage in TEM to synthesize magnetic metal nanoparticles from a MOF

Dan Xu; Daliang Zhang; Houbing Zou; Liangkui Zhu; Ming Xue; Qianrong Fang; Shilun Qiu

doi:10.1039/C6CC05366A

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Guidance from an in situ hot stage in TEM to synthesize magnetic metal nanoparticles from a MOF†

Dan Xu,^a Daliang Zhang,*^a Houbing Zou,^a Liangkui Zhu,^a Ming Xue,^a Qianrong Fang*^a and Shilun Qiu^a

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* Corresponding authors

^a State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun 130012, P. R. China
E-mail: qrfang@jlu.edu.cn, zhangdaliang@jlu.edu.cn

Abstract

A series of in situ hot stage experiments using transmission electron microscopy (TEM) were studied to directly observe the transition of a Ni-MOF to Ni nanoparticles wrapped in carbon (Ni-NPC) over temperatures ranging from ambient temperature to 700 °C. Ni-NPC-600 displays high catalytic activity in 4-nitrophenol reduction and high conversion, even after 10 cycles.

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DOI: https://doi.org/10.1039/C6CC05366A
Article type: Communication
Submitted: 28 Jun 2016
Accepted: 21 Jul 2016
First published: 21 Jul 2016

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Chem. Commun., 2016,52, 10513-10516

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Guidance from an in situ hot stage in TEM to synthesize magnetic metal nanoparticles from a MOF

D. Xu, D. Zhang, H. Zou, L. Zhu, M. Xue, Q. Fang and S. Qiu, Chem. Commun., 2016, 52, 10513 DOI: 10.1039/C6CC05366A

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Chemical Communications

Guidance from an in situ hot stage in TEM to synthesize magnetic metal nanoparticles from a MOF†

Abstract

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Guidance from an in situ hot stage in TEM to synthesize magnetic metal nanoparticles from a MOF

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