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Issue 6, 2015
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Oxidative cross S–H/S–H coupling: selective synthesis of unsymmetrical aryl tert-alkyl disulfanes

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Abstract

Selective oxidative coupling between aryl and tert-alkyl mercaptans was achieved using tert-butyl hydroperoxide (TBHP) as the oxidant and N-iodosuccinimide (NIS) as a catalyst. This protocol may provide an efficient process to synthesize unsymmetrical aryl tert-alkyl disulfanes.

Graphical abstract: Oxidative cross S–H/S–H coupling: selective synthesis of unsymmetrical aryl tert-alkyl disulfanes

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Publication details

The article was received on 23 Jan 2015, accepted on 25 Mar 2015 and first published on 25 Mar 2015


Article type: Research Article
DOI: 10.1039/C5QO00027K
Citation: Org. Chem. Front., 2015,2, 677-680
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    Oxidative cross S–H/S–H coupling: selective synthesis of unsymmetrical aryl tert-alkyl disulfanes

    J. Yuan, C. Liu and A. Lei, Org. Chem. Front., 2015, 2, 677
    DOI: 10.1039/C5QO00027K

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