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Issue 70, 2015
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Sealed rotors for in situ high temperature high pressure MAS NMR

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Abstract

Here we present the design of reusable and perfectly sealed all-zirconia MAS rotors. The rotors are used to study AlPO4-5 molecular sieve crystallization under hydrothermal conditions, high temperature high pressure cyclohexanol dehydration reaction, and low temperature metabolomics of intact biological tissue.

Graphical abstract: Sealed rotors for in situ high temperature high pressure MAS NMR

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Publication details

The article was received on 11 May 2015, accepted on 06 Jul 2015 and first published on 06 Jul 2015


Article type: Communication
DOI: 10.1039/C5CC03910J
Citation: Chem. Commun., 2015,51, 13458-13461
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    Sealed rotors for in situ high temperature high pressure MAS NMR

    J. Z. Hu, M. Y. Hu, Z. Zhao, S. Xu, A. Vjunov, H. Shi, D. M. Camaioni, C. H. F. Peden and J. A. Lercher, Chem. Commun., 2015, 51, 13458
    DOI: 10.1039/C5CC03910J

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