Issue 26, 2015
From the journal:

Chemical Communications

One hydrogen bond does not a separation make, or does it? Resolution of amines by diacetoneketogulonic acid†

Nikoletta B. Báthori,*a   Luigi R. Nassimbenia  and  Jacco van de Streekb  

* Corresponding authors

a Crystal Engineering Unit, Department of Chemistry, Faculty of Applied Sciences, Cape Town, South Africa
E-mail: bathorin@cput.ac.za
Fax: +27 21 460 3854
Tel: +27 21 460 8354

b Department of Pharmacy, University of Copenhagen, Universitetsparken 2, 2100 Copenhagen, Denmark

Abstract

Diacetoneketogulonic acid was used to separate primary amines from their racemic modifications and the selectivity of the acid was rationalized by lattice energy calculations and analyzing the weak interactions around the captured amines.

Graphical abstract: One hydrogen bond does not a separation make, or does it? Resolution of amines by diacetoneketogulonic acid

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Article information

DOI
https://doi.org/10.1039/C5CC00440C
Article type
Communication
Submitted
16 Jan 2015
Accepted
13 Feb 2015
First published
17 Feb 2015

Chem. Commun., 2015,51, 5664-5667

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One hydrogen bond does not a separation make, or does it? Resolution of amines by diacetoneketogulonic acid

N. B. Báthori, L. R. Nassimbeni and J. van de Streek, Chem. Commun., 2015, 51, 5664 DOI: 10.1039/C5CC00440C

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