Capping of cyclotriphenolene (3a) by the more available cyclotriguaiacylene (3c) or trisbromocyclotriphenolene (3b) gives the first rim-functionalized cryptophane-111 derivatives. Crystal structures of the xenon complexes reveal high cavity packing coefficients and unprecedentedly short Xe⋯C contacts.
A. I. Joseph, G. El-Ayle, C. Boutin, E. Léonce, P. Berthault and K. T. Holman, Chem. Commun., 2014, 50, 15905 DOI: 10.1039/C4CC08001G
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