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Issue 92, 2014
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A facile single crystal to single crystal transition with significant structural contraction on desolvation

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Abstract

5-Ethynyl-1,3-benzenedicarboxylic acid (H2ebdc) reacted with lead(II) acetate trihydrate yields a 1D ladder network, [Pb(ebdc)(MeOH)]2·H2O (1). Removing crystals of 1 from the mother liquor results in a facile single crystal to single crystal transition, yielding 2D [Pb(ebdc)] net (2) with a change in space group from I2/a to P[1 with combining macron].

Graphical abstract: A facile single crystal to single crystal transition with significant structural contraction on desolvation

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Publication details

The article was received on 21 Aug 2014, accepted on 26 Sep 2014 and first published on 01 Oct 2014


Article type: Communication
DOI: 10.1039/C4CC06587E
Citation: Chem. Commun., 2014,50, 14436-14439
  • Open access: Creative Commons BY license
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    A facile single crystal to single crystal transition with significant structural contraction on desolvation

    J. V. Knichal, W. J. Gee, A. D. Burrows, P. R. Raithby, S. J. Teat and C. C. Wilson, Chem. Commun., 2014, 50, 14436
    DOI: 10.1039/C4CC06587E

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