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Issue 15, 2015
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Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

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Abstract

A rapid NMR data acquisition strategy in terms of enhanced resolution per time unit for the simple and efficient determination of multiple coupling constants is described. The use of 13C spectral aliasing combined by broadband 1H homodecoupling allows accurate measurements from ultra high resolved 2D HSQC cross-peaks.

Graphical abstract: Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

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Publication details

The article was received on 23 Dec 2014, accepted on 14 Jan 2015 and first published on 14 Jan 2015


Article type: Communication
DOI: 10.1039/C4CC10279G
Author version available: Download Author version (PDF)
Citation: Chem. Commun., 2015,51, 3262-3265
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    Ultra high-resolution HSQC: application to the efficient and accurate measurement of heteronuclear coupling constants

    N. Marcó, A. Fredi and T. Parella, Chem. Commun., 2015, 51, 3262
    DOI: 10.1039/C4CC10279G

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