Issue 16, 2013

N-Bromosuccinimide–carboxylic acid combination: mild and efficient access to dibromination of unsaturated carbonyl compounds

Abstract

A mild, efficient and practical method for the preparation of dihalogenated products has been developed. Benzoic acid (0.2 equiv.) is capable of catalyzing the reactions of unsaturated carbonyl compounds with N-halosuccinimides (NXS, X = Br and Cl) to afford a series of dihalogenated products at room temperature.

Graphical abstract: N-Bromosuccinimide–carboxylic acid combination: mild and efficient access to dibromination of unsaturated carbonyl compounds

Supplementary files

Article information

Article type
Communication
Submitted
23 Jan 2013
Accepted
12 Feb 2013
First published
13 Feb 2013

RSC Adv., 2013,3, 5382-5385

N-Bromosuccinimide–carboxylic acid combination: mild and efficient access to dibromination of unsaturated carbonyl compounds

H. Xue, H. Tan, D. Wei, Y. Wei, S. Lin, F. Liang and B. Zhao, RSC Adv., 2013, 3, 5382 DOI: 10.1039/C3RA40360B

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