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Issue 8, 2013
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Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

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Abstract

The synthesis of a new mesoporous BTD-COF based on a transesterification reaction was carried out in a two step microwave synthesis procedure in only 40 min: first the pinacolboronate 4,7-bis[4-(4,4,5,5)-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzo[1,2,5]-thiadiazole (BTDBE) was cleaved with HCl, in a second step addition of hexahydroxytriphenylene (HHTP) resulted in the growth of the crystalline framework with high surface area and a pore size of about 4 nm.

Graphical abstract: Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

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Publication details

The article was received on 21 Aug 2012, accepted on 21 Nov 2012 and first published on 22 Nov 2012


Article type: Communication
DOI: 10.1039/C2CE26343B
Citation: CrystEngComm, 2013,15, 1500-1502
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    Facile synthesis of a mesoporous benzothiadiazole-COF based on a transesterification process

    M. Dogru, A. Sonnauer, S. Zimdars, M. Döblinger, P. Knochel and T. Bein, CrystEngComm, 2013, 15, 1500
    DOI: 10.1039/C2CE26343B

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