Department of Mechanical Engineering, University of Connecticut, 191 Auditorium Road, Unit 3139, Storrs, USA
; Tel: +860-486-3647
Center for Innovative Fuel Cell and Battery Technologies, School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta, USA
; Tel: +404-894-6114
Advanced Photon Source, Argonne National Laboratory, Building 401, 9700 South Cass Avenue, Argonne, USA
; Tel: +630-252-3789
NSLS-II, Brookhaven National Laboratory, Upton, USA
; Tel: +631-344-5582
Nanoscale, 2012,4, 1557-1560
09 Nov 2011,
06 Jan 2012
First published online
10 Jan 2012
Nano-structures of nickel (Ni) and nickel subsulfide (Ni3S2) materials were studied and mapped in 3D with high-resolution x-ray nanotomography combined with full field XANES spectroscopy. This method for characterizing these phases in complex microstructures is an important new analytical imaging technique, applicable to a wide range of nanoscale and mesoscale electrochemical systems.
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